N-NITROSOMETHYL-2-CHLOROETHYLAMINE

Base Information

• Chemical Name: N-NITROSOMETHYL-2-CHLOROETHYLAMINE
• CAS No.: 16339-16-5
• Molecular Formula: C₃H₇ClN₂O
• Molecular Weight: 122.554
• Hs Code.: 2928000090
• Mol file: 16339-16-5.mol

Synonyms:Ethylamine,2-chloro-N-methyl-N-nitroso- (6CI,8CI); (2-Chloroethyl)methylnitrosamine;2-Chloro-N-methyl-N-nitrosoethylamine; Methyl-2-chloroethylnitrosamine;N-Nitroso-N-methyl-2-chloroethylamine; N-Nitrosomethyl-2-chloroethylamine; NSC3370

Chemical Property of N-NITROSOMETHYL-2-CHLOROETHYLAMINE

Chemical Property:

• Vapor Pressure: 0.0927mmHg at 25°C
• Refractive Index: 1.4510 (estimate)
• Boiling Point: 231.8°Cat760mmHg
• Flash Point: 94°C
• PSA: 32.67000
• Density: 1.2g/cm³
• LogP: 0.83840

Purity/Quality:

99% ^*data from raw suppliers

N-NITROSOMETHYL-2-CHLOROETHYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-NITROSOMETHYL-2-CHLOROETHYLAMINE

There total 3 articles about N-NITROSOMETHYL-2-CHLOROETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hydroxy-[3-(2-hydroxyethyl)-3-methyl]-1-triazene 2-oxide sodium salt (742081-66-9) + 3-(2-chloroethyl)-1-chloromethoxy-3-methyltriaz-1-ene 2-oxide → N-Nitroso-methyl-2-chloraethylamin (16339-16-5) + N-(2-hydroxyethyl)-N-methyl-N-nitrosamine (26921-68-6)

Guidance literature:

With sodium carbonate; In acetonitrile; at 0 - 20 ℃; for 7h;

DOI:10.1007/s11172-015-1211-0

Reference yield:

→ N-Nitroso-methyl-2-chloraethylamin (16339-16-5)

Guidance literature:

With acetic acid; sodium nitrite;

Reference yield:

→ N-Nitroso-methyl-2-chloraethylamin (16339-16-5)

Guidance literature:

β-Hydroxyethyl-methyl-nitrosamin, Bzl., 1.) SOCl2, -10 bis -15grad, 2.) Na2CO3, Kochen, 3 h;

DOI:10.1021/jo01064a610

upstream raw materials:

1-hydroxy-[3-(2-hydroxyethyl)-3-methyl]-1-triazene 2-oxide sodium salt

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