<1S-<1α,2α(Z),3α(E,3S^*,4R^*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid

Base Information

• Chemical Name: <1S-<1α,2α(Z),3α(E,3S^*,4R^*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid
• CAS No.: 126295-62-3
• Molecular Formula: C₂₆H₃₆O₄
• Molecular Weight: 412.569

Synonyms:<1S-<1α,2α(Z),3α(E,3S^*,4R^*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid

Chemical Property of <1S-<1α,2α(Z),3α(E,3S^*,4R^*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid

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Technology Process of <1S-<1α,2α(Z),3α(E,3S^*,4R^*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid

There total 2 articles about <1S-<1α,2α(Z),3α(E,3S^*,4R^*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-7-[(1S,2R,3S,4R)-3-((E)-(3R,4S)-3-Hydroxy-4-phenyl-pent-1-enyl)-7-oxa-bicyclo[2.2.1]hept-2-yl]-2,2-dimethyl-hept-5-enoic acid methyl ester → <1S-<1α,2α(Z),3α(E,3S*,4R*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid (126295-62-3)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; at 25 ℃; for 96h;

DOI:10.1021/jm00168a032

Reference yield:

(Z)-2,2-Dimethyl-7-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hept-5-enoic acid methyl ester (126295-61-2) → <1S-<1α,2α(Z),3α(E,3S*,4R*),4α>>-2,2-dimethyl-7-<3-(3-hydroxy-4-phenyl-1-pentenyl)-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoic acid (126295-62-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 N aq. HCl / tetrahydrofuran / 18 h / 25 °C

2: 1 N aq. LiOH / tetrahydrofuran / 96 h / 25 °C

With hydrogenchloride; lithium hydroxide; In tetrahydrofuran;

DOI:10.1021/jm00168a032

upstream raw materials:

(Z)-2,2-Dimethyl-7-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hept-5-enoic acid methyl ester

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