2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

Base Information

Chemical Name:2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid
CAS No.:1065496-93-6
Molecular Formula:C₃₇H₄₂O₁₀
Molecular Weight:646.734
Hs Code.:

Synonyms:2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

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Chemical Property of 2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

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Technology Process of 2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

There total 3 articles about 2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1065496-91-4
methyl 2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoate

: 1065496-93-6
2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

Guidance literature:: With potassium hydroxide; In methanol; water; at 20 ℃; for 144h; Inert atmosphere;
DOI:10.1248/cpb.c12-00365

Reference yield:

: 431049-86-4
tert-butyl 5-formyl-2-hydroxybenzoate

: 1065496-93-6
2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 1 h / 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: potassium hydroxide / methanol; water / 144 h / 20 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; potassium hydroxide; In tetrahydrofuran; methanol; water; acetone;
DOI:10.1248/cpb.c12-00365

Reference yield:

: 1065496-85-6
methyl 2,5-bis((diethoxyphosphoryl)methyl)benzoate

: 1065496-89-0
tert-butyl 5-formyl-2-(methoxymethoxy)benzoate

: 1065496-93-6
2,5-bis((E)-3-(tert-butoxycarbonyl)-4-(methoxymethoxy)styryl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

2.1: potassium hydroxide / methanol; water / 144 h / 20 °C / Inert atmosphere

With potassium tert-butylate; potassium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1248/cpb.c12-00365