3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Base Information

Chemical Name:3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene
CAS No.:103723-88-2
Molecular Formula:C₁₄H₁₉NO₃
Molecular Weight:249.31
Hs Code.:

Synonyms:3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

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Chemical Property of 3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

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Technology Process of 3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

There total 3 articles about 3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 103723-87-1
3,4-dimethylcyclohex-3-enyl N-hydroxycarbamate

: 103723-88-2
3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: With hydrogenchloride; sodium periodate; sodium acetate; In water; ethyl acetate; at 0 ℃; for 1h;

Reference yield:

: 53829-23-5
3,4-dimethylcyclohex-3-enol

: 103723-88-2
3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3 h / 0 °C

2: hydroxylamine hydrochloride, sodium hydroxide / H₂O / 1 h / Ambient temperature

3: 79 percent / sodium periodate, sodium acetate, hydrochloric acid / H₂O; ethyl acetate / 1 h / 0 °C

With hydrogenchloride; sodium hydroxide; sodium periodate; hydroxylamine hydrochloride; sodium acetate; In water; ethyl acetate; toluene;

Reference yield:

: 103723-86-0
C₉H₁₃ClO₂

: 103723-88-2
3-(3,4-dimethylcyclohex-3-enyloxycarbonyl)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride, sodium hydroxide / H₂O / 1 h / Ambient temperature

2: 79 percent / sodium periodate, sodium acetate, hydrochloric acid / H₂O; ethyl acetate / 1 h / 0 °C

With hydrogenchloride; sodium hydroxide; sodium periodate; hydroxylamine hydrochloride; sodium acetate; In water; ethyl acetate;