2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione

Base Information

• Chemical Name: 2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione
• CAS No.: 164164-29-8
• Molecular Formula: C₃₀H₂₆N₂O₄
• Molecular Weight: 478.547

Synonyms:2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione

Chemical Property of 2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione

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Technology Process of 2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione

There total 1 articles about 2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-Fluoro-biphenyl-3-carboxylic acid (2-hydroxy-ethyl)-amide → 2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione (164164-29-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1016/0040-4039(94)02345-C

Reference yield: 73.0%

2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione (164164-29-8) → 2,11-Diphenyl-6,7,8,9,15,16,17,18-octahydro-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; benzene;

DOI:10.1016/0040-4039(94)02345-C

Reference yield:

2,11-Diphenyl-7,8,16,17-tetrahydro-6H,15H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecene-9,18-dione (164164-29-8) → (17-Cyanomethyl-2,11-diphenyl-6,7,15,16,17,18-hexahydro-9H-5,14-dioxa-8,17-diaza-dibenzo[a,h]cyclotetradecen-8-yl)-acetonitrile

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / LiAlH₄ / diethyl ether; benzene

2: 68 percent / NaH / tetrahydrofuran / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; diethyl ether; benzene;

DOI:10.1016/0040-4039(94)02345-C

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