C₃₀H₄₇NO₆

Base Information

Chemical Name:C₃₀H₄₇NO₆
CAS No.:1302981-71-0
Molecular Formula:C₃₀H₄₇NO₆
Molecular Weight:517.706
Hs Code.:

C<sub>30</sub>H<sub>47</sub>NO<sub>6</sub>

Synonyms:C₃₀H₄₇NO₆

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Chemical Property of C₃₀H₄₇NO₆

Chemical Property:

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Technology Process of C₃₀H₄₇NO₆

There total 14 articles about C₃₀H₄₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₄₉NO₇

: 1302981-71-0
C₃₀H₄₇NO₆

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2010.11.012

Reference yield:

: 1302981-73-2
C₃₁H₄₀O₄Si

: 1302981-71-0
C₃₀H₄₇NO₆

Guidance literature:: Multi-step reaction with 14 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2.1: chloro-trimethyl-silane; lithium diisopropyl amide / tetrahydrofuran

2.2: 12 h / Reflux

4.1: tetrabutyl ammonium fluoride

5.1: pyridine

6.1: potassium tert-butylate

7.1: lithium aluminium tetrahydride / diethyl ether / -20 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane

9.1: tetrahydrofuran / -78 °C

10.1: dmap / dichloromethane

11.1: diisobutylaluminium hydride / -78 °C

12.1: sodium hydrogencarbonate; Dess-Martin periodane

13.1: potassium fluoride / isopropyl alcohol / 24 h / 22 °C

14.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.17 h / 0 °C

With pyridine; dmap; potassium fluoride; lithium aluminium tetrahydride; chloro-trimethyl-silane; potassium tert-butylate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; isopropyl alcohol; 2.1: Claisen rearrangement / 2.2: Claisen rearrangement / 8.1: Dess-Martin oxidation / 9.1: Aldol condensation / 12.1: Dess-Martin oxidation / 13.1: Henry reaction;
DOI:10.1016/j.tetlet.2010.11.012

Reference yield:

: 1302981-74-3
C₄₁H₅₈O₅Si

: 1302981-71-0
C₃₀H₄₇NO₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: chloro-trimethyl-silane; lithium diisopropyl amide / tetrahydrofuran

1.2: 12 h / Reflux

3.1: tetrabutyl ammonium fluoride

4.1: pyridine

5.1: potassium tert-butylate

6.1: lithium aluminium tetrahydride / diethyl ether / -20 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane

8.1: tetrahydrofuran / -78 °C

9.1: dmap / dichloromethane

10.1: diisobutylaluminium hydride / -78 °C

11.1: sodium hydrogencarbonate; Dess-Martin periodane

12.1: potassium fluoride / isopropyl alcohol / 24 h / 22 °C

13.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.17 h / 0 °C

With pyridine; dmap; potassium fluoride; lithium aluminium tetrahydride; chloro-trimethyl-silane; potassium tert-butylate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; isopropyl alcohol; 1.1: Claisen rearrangement / 1.2: Claisen rearrangement / 7.1: Dess-Martin oxidation / 8.1: Aldol condensation / 11.1: Dess-Martin oxidation / 12.1: Henry reaction;
DOI:10.1016/j.tetlet.2010.11.012