5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one

Base Information

• Chemical Name: 5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one
• CAS No.: 515114-47-3
• Molecular Formula: C₁₈H₂₁N₃O
• Molecular Weight: 297.362

Synonyms:5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one

Chemical Property of 5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one

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Technology Process of 5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one

There total 1 articles about 5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-[3-cyano-4,5-dimethyl-1-(2,4,6-trimethylphenyl)-1H-pyrrol-2-yl][13C2]acetamide (515114-46-2) → 5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one (515114-47-3)

Guidance literature:

With phosphoric acid; In acetic acid; at 120 ℃;

DOI:10.1002/jlcr.576

Reference yield: 91.3%

5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one (515114-47-3) → 4-chloro-5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d][2-13C]pyrimidine

Guidance literature:

With trichlorophosphate; Heating;

DOI:10.1002/jlcr.576

Reference yield:

5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-3,7-dihydropyrrolo[2,3-d][2-13C]pyrimidin-4-one (515114-47-3) → butyl-ethyl-[5,6-dimethyl-2-[13C]methyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d][2-13C]pyrimidin-4-yl]-amine

Guidance literature:

Multi-step reaction with 2 steps

1: 91.3 percent / phosphorus oxychloride / Heating

2: 80 percent / dimethylsulfoxide / 135 °C

With trichlorophosphate; In dimethyl sulfoxide;

DOI:10.1002/jlcr.576

upstream raw materials:

N-[3-cyano-4,5-dimethyl-1-(2,4,6-trimethylphenyl)-1H-pyrrol-2-yl][13C₂]acetamide

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