4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

Base Information

Chemical Name:4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate
CAS No.:1345002-90-5
Molecular Formula:C₃₃H₃₈FNO₆
Molecular Weight:563.666
Hs Code.:

Synonyms:4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

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Technology Process of 4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

There total 8 articles about 4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1345003-09-9
C₁₄H₁₇FO₃

: 166331-73-3
4-((R)-1-methylhexyloxy)-3-nitro-4'-hydroxybiphenyl

: 1345002-90-5
4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

Guidance literature:: C₁₄H₁₇FO₃; 4-((R)-1-methylhexyloxy)-3-nitro-4'-hydroxybiphenyl; With dmap; In dichloromethane;

With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1080/15421406.2011.570148

Reference yield:

: 92-88-6
4,4'-Dihydroxybiphenyl

: 1345002-90-5
4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: nitric acid

3: triphenylphosphine; diethylazodicarboxylate

4: water; lithium hydroxide

5: dmap / dichloromethane

With pyridine; dmap; water; nitric acid; triphenylphosphine; lithium hydroxide; diethylazodicarboxylate; In dichloromethane;
DOI:10.1080/15421406.2011.570148

Reference yield:

: 166331-72-2
4'-((R)-1-methylhexyloxy)-3'-nitro-4-biphenylyl benzoate

: 1345002-90-5
4'-((R)-2-heptyloxy)-3'-nitro-4-biphenylyl 4-(6-heptenyloxy)-3-fluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide

2: dmap / dichloromethane

With dmap; water; lithium hydroxide; In dichloromethane;
DOI:10.1080/15421406.2011.570148