(2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

Base Information

Chemical Name:(2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate
CAS No.:1579963-96-4
Molecular Formula:C₂₀H₂₀N₂O₇S
Molecular Weight:432.454
Hs Code.:

Synonyms:(2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

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Chemical Property of (2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

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Technology Process of (2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

There total 7 articles about (2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1579963-98-6
(2E,4E)-methyl 6-(N-(2-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

: 1579963-96-4
(2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/chem.201303435

Reference yield:

: 110-44-1,91751-55-2
sorbic Acid

: 1579963-96-4
(2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 2 h / -10 °C / Reflux; Inert atmosphere

2: N-Bromosuccinimide; dibenzoyl peroxide / water / 1.5 h / Reflux; Inert atmosphere

3: potassium carbonate / acetonitrile / 2 h / 60 °C / Inert atmosphere

4: acetic acid / water; tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; thionyl chloride; potassium carbonate; acetic acid; dibenzoyl peroxide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1002/chem.201303435

Reference yield:

: 689-89-4
(2E,4E)-methylhexa-2,4-dienoate

: 1579963-96-4
(2E,4E)-methyl 6-(N-(2-(hydroxymethyl)phenyl)-4-nitrophenylsulfonamido)hexa-2,4-dienoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / water / 1.5 h / Reflux; Inert atmosphere

2: potassium carbonate / acetonitrile / 2 h / 60 °C / Inert atmosphere

3: acetic acid / water; tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; acetic acid; dibenzoyl peroxide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1002/chem.201303435