1-nitroso-3-chloro-3-phenylazetidine

Base Information

• Chemical Name: 1-nitroso-3-chloro-3-phenylazetidine
• CAS No.: 156908-55-3
• Molecular Formula: C₉H₉ClN₂O
• Molecular Weight: 196.636
• Mol file: 156908-55-3.mol

Synonyms:1-nitroso-3-chloro-3-phenylazetidine

Chemical Property of 1-nitroso-3-chloro-3-phenylazetidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-nitroso-3-chloro-3-phenylazetidine

There total 2 articles about 1-nitroso-3-chloro-3-phenylazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Chlor-3-phenylazetidinhydrochlorid (35903-75-4) → 1-nitroso-3-chloro-3-phenylazetidine (156908-55-3)

Guidance literature:

With n-Butyl nitrite; In chloroform; Yield given; Ambient temperature;

Reference yield:

3-phenyl-1-azabicyclo[1.1.0]butane (17945-94-7) → 1-nitroso-3-chloro-3-phenylazetidine (156908-55-3)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / diethyl ether / 0.5 h / -30 °C

2: BuONO / CHCl₃ / Ambient temperature

With hydrogenchloride; n-Butyl nitrite; In diethyl ether; chloroform;

Reference yield: 96.0%

1-nitroso-3-chloro-3-phenylazetidine (156908-55-3) → 1-chlorostyrene (618-34-8)

Guidance literature:

at 400 ℃; under 0.002 Torr;

upstream raw materials:

3-Chlor-3-phenylazetidinhydrochlorid

3-phenyl-1-azabicyclo[1.1.0]butane

Downstream raw materials:

1-chlorostyrene

Refernces