3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

Base Information

Chemical Name:3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide
CAS No.:76927-62-3
Molecular Formula:C₃₀H₃₄N₄O₉
Molecular Weight:594.621
Hs Code.:

Synonyms:3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

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Chemical Property of 3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

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Technology Process of 3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

There total 17 articles about 3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 78217-78-4
N⁴--N¹,N⁸-bis(2,3-dimethoxybenzoyl)spermidine

: 76927-62-3
3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

Guidance literature:: With boron tribromide; In dichloromethane; for 18h; 0 deg C to room temperature;
DOI:10.1021/jo00335a041

Reference yield: 47.0%

: 161219-95-0
N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

: 76927-62-3
3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

Guidance literature:: With palladium hydroxide - carbon; In ethanol; cyclohexene; for 3h; Heating;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 73038-05-8
N-(3-aminobutyl)-N-(3-aminopropyl)(phenylmethyl)amine

: 76927-62-3
3-<(2,3-dihydroxybenzoylamino)propyl>-N-<4-(2,3-dihydroxy-benzoylamino)butyl>-2-hydroxybenzoyl-glycylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / triethylamine / CH₂Cl₂ / 18 h / 0 deg C to room temperature

2: 98 percent / 1) H₂, 2) NaOMe / 1) PdCl₂ / 1) glacial acetic acid, room temperature, 2) MeOH, 30 min

3: 95 percent / triethylamine / CH₂Cl₂ / 40 h / -78 deg C to room temperature

4: 97 percent / BBr₃ / CH₂Cl₂ / 18 h / 0 deg C to room temperature

With hydrogen; sodium methylate; boron tribromide; triethylamine; palladium dichloride; In dichloromethane;
DOI:10.1021/jo00335a041