Technology Process of 3,5-dimethoxy-4-methylthiobenzaldehyde
There total 5 articles about 3,5-dimethoxy-4-methylthiobenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C11H14O4S; dimethyl sulfate;
In
methanol;
at 55 ℃;
for 1h;
Inert atmosphere;
With
hydrogenchloride;
In
methanol; water;
for 2h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2017.11.050
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diphenylether / 0.25 h / 240 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / toluene / 2.5 h / 145 °C
3.1: potassium hydroxide / methanol / 3 h / 80 °C / Inert atmosphere
4.1: methanol / 1 h / 55 °C / Inert atmosphere
4.2: 2 h / Inert atmosphere
With
toluene-4-sulfonic acid; potassium hydroxide;
In
methanol; diphenylether; toluene;
1.1: |Newman-Kwart Rearrangement;
DOI:10.1016/j.ejmech.2017.11.050
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide / water; tetrahydrofuran / 0.83 h / 0 - 20 °C
2.1: diphenylether / 0.25 h / 240 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / toluene / 2.5 h / 145 °C
4.1: potassium hydroxide / methanol / 3 h / 80 °C / Inert atmosphere
5.1: methanol / 1 h / 55 °C / Inert atmosphere
5.2: 2 h / Inert atmosphere
With
toluene-4-sulfonic acid; potassium hydroxide;
In
tetrahydrofuran; methanol; diphenylether; water; toluene;
2.1: |Newman-Kwart Rearrangement;
DOI:10.1016/j.ejmech.2017.11.050
