Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

Base Information

Chemical Name:Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate
CAS No.:140156-82-7
Molecular Formula:C₂₅H₂₄N₂O₅
Molecular Weight:432.476
Hs Code.:

Synonyms:Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

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Chemical Property of Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

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Technology Process of Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

There total 1 articles about Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.4%

: 6780-38-7
N-phthaloylglycine chloride

: 140156-76-9
Triallyl 1,1',1''-(Hexahydro-1,3,5-triazine-1,3,5-triyl)tris(cyclopentanecarboxylate)

: 140156-82-7
Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

Guidance literature:: With pyridine; boron trifluoride diethyl etherate; In dichloromethane; at -75 ℃; for 3h;

Reference yield: 79.0%

: 140156-82-7
Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

: 140156-85-0
1-(3-Amino-2-oxo-azetidin-1-yl)-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: With methylhydrazine; In dichloromethane; for 8h; Ambient temperature;

Reference yield:

: 140156-82-7
Benzyl 1-(2-Oxo-3-phthalimidoazetidin-1-yl)cyclohexanecarboxylate

: 140156-93-0
1-{3-[2-(3-Chloro-isoxazol-5-yl)-acetylamino]-2-oxo-azetidin-1-yl}-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / MeNHNH₂ / CH₂Cl₂ / 8 h / Ambient temperature

2: 68 percent / DCC, 1-hydroxybenzotriazole / dimethylformamide / 1-2 d

3: 77 percent / 10percent Pd-C / ethyl acetate

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; methylhydrazine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;