Technology Process of C30H36O5
There total 7 articles about C30H36O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; water; 4-methylmorpholine N-oxide;
In
tetrahydrofuran;
at 20 ℃;
for 17h;
DOI:10.1021/ol300182r
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Dess-Martin periodane / dichloromethane / 5 h / 0 °C
2.1: toluene / -78 °C / Molecular sieve
2.2: 0.5 h / 0 °C
3.1: pyridine; dmap / dichloromethane
4.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 17 h / 20 °C
With
pyridine; dmap; osmium(VIII) oxide; water; Dess-Martin periodane; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; toluene;
1.1: Dess-Martin oxidation / 2.1: Roush coupling / 2.2: Roush coupling;
DOI:10.1021/ol300182r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C
2.1: Dess-Martin periodane / dichloromethane / 5 h / 0 °C
3.1: toluene / -78 °C / Molecular sieve
3.2: 0.5 h / 0 °C
4.1: pyridine; dmap / dichloromethane
5.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 17 h / 20 °C
With
pyridine; dmap; osmium(VIII) oxide; tetrabutyl ammonium fluoride; water; Dess-Martin periodane; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; toluene;
2.1: Dess-Martin oxidation / 3.1: Roush coupling / 3.2: Roush coupling;
DOI:10.1021/ol300182r
