2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Base Information

Chemical Name:2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester
CAS No.:794588-63-9
Molecular Formula:C₂₆H₃₂O₅
Molecular Weight:424.537
Hs Code.:

Synonyms:2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

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Chemical Property of 2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

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Technology Process of 2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

There total 2 articles about 2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 61436-73-5
2-allylbenzoic acid

: 794588-45-7
1-allyloxy-5-(4-methoxybenzyloxy)pentan-3-ol

: 794588-63-9
2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In diethyl ether; at 0 - 20 ℃;
DOI:10.1016/j.tet.2004.06.146

Reference yield:

: 794588-83-3
(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)pentan-1-ol

: 794588-63-9
2-allylbenzoic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaH / tetrahydrofuran / 20 h / 20 °C

2: 74 percent / TBAF / tetrahydrofuran / 5 h / 20 °C

3: 97 percent / diisopropyl azodicarboxylate; PPh₃ / diethyl ether / 0 - 20 °C

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; 3: Mitsunobu reaction;
DOI:10.1016/j.tet.2004.06.146