3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

Base Information

Chemical Name:3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid
CAS No.:400859-83-8
Molecular Formula:C₁₆H₂₀FN₃O₆S
Molecular Weight:401.416
Hs Code.:

Synonyms:3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

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Chemical Property of 3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

Chemical Property:

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Technology Process of 3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

There total 1 articles about 3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3895-25-8
4-fluorophenylsulfonyl isocyanate

: 3-[((S)-Piperidine-2-carbonyl)-amino]-propionic acid

: 400859-83-8
3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

Guidance literature:: In acetonitrile; at 4 ℃;
DOI:10.1021/jm010958k

Reference yield:

: 400859-11-2
N-1-tritylsulfenyl-L-histidine tert-butyl ester

: 400859-83-8
3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

: 400860-69-7
2-(3-{[1-(4-fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionylamino)-3-(1-tritylsulfanyl-1H-imidazol-4-yl)-propionic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; diisopropyl-carbodiimide; In acetonitrile; at 4 ℃;
DOI:10.1021/jm010958k

Reference yield:

: 400859-83-8
3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionic acid

: (S)-2-(3-{[(S)-1-(4-Fluoro-benzenesulfonylaminocarbonyl)-piperidine-2-carbonyl]-amino}-propionylamino)-3-(1H-imidazol-4-yl)-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropyl-carbodiimide; 1-hydroxybenzotriazole / acetonitrile / 4 °C

2: HCl / dioxane / 40 °C

With hydrogenchloride; benzotriazol-1-ol; diisopropyl-carbodiimide; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jm010958k