4-cyclohexylidenebutyl acetate

Base Information

Chemical Name:4-cyclohexylidenebutyl acetate
CAS No.:36144-20-4
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:

Synonyms:4-cyclohexylidenebutyl acetate

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Chemical Property of 4-cyclohexylidenebutyl acetate

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Technology Process of 4-cyclohexylidenebutyl acetate

There total 3 articles about 4-cyclohexylidenebutyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1576-85-8
4-pentenyl acetate

: 1192-37-6
methylenecyclohexane

: 36144-20-4
4-cyclohexylidenebutyl acetate

Guidance literature:: N-heterocyclic carbene ligand-based ruthenium catalyst; In dichloromethane; for 24h; Heating;
DOI:10.1021/ol702624n

Reference yield: 74.0%

: 1121-49-9
bromomethylenecyclohexane

: triethylammonium 3-acetoxypropylbis(catecholato)silicate

: 36144-20-4
4-cyclohexylidenebutyl acetate

Guidance literature:: With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; (1,2-dimethoxyethane)dichloronickel(II); 4,4'-di-tert-butyl-2,2'-bipyridine; In N,N-dimethyl-formamide; at 27 ℃; for 24h; Sealed tube; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.6b00024

Reference yield: 55.0%

: 1121-49-9
bromomethylenecyclohexane

: potassium [18-crown-6] bis(catecholato)acetoxypropylsilicate

: 36144-20-4
4-cyclohexylidenebutyl acetate

Guidance literature:: With [nickel(II)dichloride(dimethoxyethane)]; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; 4,4'-di-tert-butyl-2,2'-bipyridine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Schlenk technique; Glovebox; Inert atmosphere; Irradiation;
DOI:10.1039/c6cc04636c