(+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

Base Information

Chemical Name:(+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine
CAS No.:136083-18-6
Molecular Formula:C₂₆H₃₂N₂O₄Si
Molecular Weight:464.637
Hs Code.:

Synonyms:(+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

Suppliers and Price of (+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

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Technology Process of (+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

There total 5 articles about (+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 116165-26-5
5-Methyl-1-trimethylsilanyl-1H-pyrimidine-2,4-dione

: 136083-14-2
(+/-)-1-tert-Butyldiphenylsilyloxy-2-acetoxymethylenoxybut-3-ene

: 136083-18-6
(+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

Guidance literature:: With dibenzo-18-crown-6; potassium iodide; In toluene; acetonitrile; at 80 ℃; for 2h; solid-liquid phase transfer catalysis;

Reference yield:

: 177032-63-2
(+/-)-1-(tert-butyldiphenylsilyloxy)-2-hydroxy-3-butene

: 136083-18-6
(+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / P₂O₅ / CHCl₃ / 24 h / Ambient temperature

2: 95 percent / BF₃*Et₂O / diethyl ether / 48 h / 4 °C

3: 90 percent / dibenzo-18-crown-6 ether, KI / acetonitrile; toluene / 2 h / 80 °C / solid-liquid phase transfer catalysis

With dibenzo-18-crown-6; boron trifluoride diethyl etherate; phosphorus pentoxide; potassium iodide; In diethyl ether; chloroform; toluene; acetonitrile;

Reference yield:

: 136083-13-1
(+/-)-1-tert-Butyldiphenylsilyloxy-2-methoxymethylenoxybut-3-ene

: 136083-18-6
(+/-)1-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>thymine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / BF₃*Et₂O / diethyl ether / 48 h / 4 °C

2: 90 percent / dibenzo-18-crown-6 ether, KI / acetonitrile; toluene / 2 h / 80 °C / solid-liquid phase transfer catalysis

With dibenzo-18-crown-6; boron trifluoride diethyl etherate; potassium iodide; In diethyl ether; toluene; acetonitrile;