(1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol

Base Information

Chemical Name:(1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol
CAS No.:128574-76-5
Molecular Formula:C₁₁H₁₈O₂
Molecular Weight:182.263
Hs Code.:

Synonyms:(1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol

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Chemical Property of (1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol

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Technology Process of (1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol

There total 1 articles about (1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33878-99-8
(S)-8a-methyl-3,4,8,8a-tetrahydro-2H,7H-naphthalene-1,6-dione

: 878-47-7,4242-00-6,34996-06-0,50302-16-4,70191-02-5,34996-05-9
(4aS,5S)-4,4a,5,6,7,8-hexahydro-5-hydroxy-4a-methylnaphthalen-2(3H)-one

: 65083-11-6,100052-83-3,118917-72-9,118918-56-2,128574-75-4,128574-76-5
8ac-Methyl-1,2,3,4,6,7,8,8a-octahydro-naphthalin-1r,6ξ-diol

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -78 ℃; Title compound not separated from byproducts;

Reference yield: 83.0%

: 128574-76-5
(1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol

: 619-84-1
p-N,N-dimethylaminobenzoic acid

: 128531-57-7
(1R,6S,8aR)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediyl bis(4-dimethylaminobenzoate)

Guidance literature:: With tributyl-amine; 2-chloro-1-methylpyridinium p-toluenesulfonate; In dichloromethane; Heating;
DOI:10.1055/s-1990-26786

Reference yield: 68.0%

: 586-76-5
4-Bromobenzoic acid

: 128574-76-5
(1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediol

: 144630-53-5
(1R,6S,8aR)-(-)-1,2,3,4,6,7,8,8a-octahydro-8a-methyl-1,6-naphthalenediyl bis(4-bromobenzoate)

Guidance literature:: With tributyl-amine; 2-chloro-1-methylpyridinium p-toluenesulfonate; In toluene; for 5h; Heating;
DOI:10.1135/cccc19921459