tris(3,5-difluorophenyl)phosphine

Base Information

Chemical Name:tris(3,5-difluorophenyl)phosphine
CAS No.:132698-61-4
Molecular Formula:C₁₈H₉F₆P
Molecular Weight:370.234
Hs Code.:

Synonyms:tris(3,5-difluorophenyl)phosphine

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Chemical Property of tris(3,5-difluorophenyl)phosphine

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Technology Process of tris(3,5-difluorophenyl)phosphine

There total 1 articles about tris(3,5-difluorophenyl)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1435-43-4
1-chloro-3,5-difluorobenzene

: 132698-61-4
tris(3,5-difluorophenyl)phosphine

Guidance literature:: With Tetrakis(dimethylamino)ethylen; phosphorus; In acetone; benzene; at 20 ℃; for 20h; Inert atmosphere; UV-irradiation; Glovebox;
DOI:10.1039/d1cc05691c

Reference yield: 20.0%

: dicarbonyl(cyclopentadienyl)methyliron(II)

: 132698-61-4
tris(3,5-difluorophenyl)phosphine

: ((C₅H₅)Fe(CO)(P(C₆H₃F₂)3)CH₃)

: ((C₅H₅)Fe(CO)(P(C₆H₃F₂)3)COCH₃)

Guidance literature:: With carbon monoxide; boron trifluoride diethyl etherate; In tetrahydrofuran; cyclohexane; Irradiation (UV/VIS); soln. of starting materials in THF/cyclohexane (under N2) is irradiated with a Hg arc lamp for 5.5 h, evapn. of solvents, addn. of THF, pressurizing with CO in a Fisher-porter bottle for 3 d; depressurizing, addn. of H2O, extn. with CH2Cl2, drying over Na2SO4, removal of volatiles under vac., chromy., elem. anal.;