4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

Base Information

Chemical Name:4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile
CAS No.:508224-22-4
Molecular Formula:C₂₃H₃₃ClN₂O₆S
Molecular Weight:501.044
Hs Code.:

Synonyms:4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

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Chemical Property of 4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

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Technology Process of 4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

There total 3 articles about 4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 508224-20-2
1,3-di[2-(2-ethoxyethoxy)ethoxy]-2-propanethiol

: 139152-08-2
4,5-dichlorophthalonitrile

: 508224-22-4
4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 50 ℃; for 48h;
DOI:10.1039/b314995a DOI:10.1039/b617773e

Reference yield:

: 1,3-di[2-(2-ethoxyethoxy)ethoxy]-2-propanol

: 508224-22-4
4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / pyridine / 48 h / 20 °C

2: 44 percent / ethanol / 48 h / Heating

3: 60 percent / K₂CO₃ / dimethylsulfoxide / 48 h / 50 °C

With potassium carbonate; In pyridine; ethanol; dimethyl sulfoxide;
DOI:10.1039/b314995a

Reference yield:

: 508224-19-9
2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-(2-ethoxyethoxy)ethoxymethyl] ethyl 4-methyl-1-benzene sulfonate

: 508224-22-4
4-chloro-5-(2-[2-(2-ethoxyethoxy)ethoxy]-1-[2-((2-ethoxyethoxy)ethoxy)ethoxymethyl]ethylsulfanyl)phthalonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / ethanol / 48 h / Heating

2: 60 percent / K₂CO₃ / dimethylsulfoxide / 48 h / 50 °C

With potassium carbonate; In ethanol; dimethyl sulfoxide;
DOI:10.1039/b314995a