(1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

Base Information

Chemical Name:(1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane
CAS No.:948049-33-0
Molecular Formula:C₁₉H₂₂N₂O₈
Molecular Weight:406.392
Hs Code.:

Synonyms:(1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

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Chemical Property of (1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

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Technology Process of (1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

There total 4 articles about (1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 948049-32-9
(1S,2R,3S,4R,5R)-3,4-diacetoxy-2-hydroxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

: 108-24-7
acetic anhydride

: 948049-33-0
(1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

Guidance literature:: With pyridine; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2007.05.085

Reference yield:

: 948049-31-8
(1S,2R,3S,4R,5R)-2,4-diacetoxy-3-benzyloxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

: 948049-33-0
(1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / Pd(OH)2 / ethanol / 1 h / atmospheric pressure

2: pyridine / CH₂Cl₂ / 0.5 h / -25 °C

3: 130.7 mg / NaNO₂ / dimethylformamide / 18 h / 20 °C

4: 90 percent / pyridine / 6 h / 20 °C

With pyridine; hydrogen; sodium nitrite; palladium dihydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.05.085

Reference yield:

: C₁₇H₂₀N₂O₇

: 948049-33-0
(1S,2R,3R,4R,5R)-2,3,4-triacetoxy-N-(N-phenylcarbamoyl)-6-oxa-nor-tropane

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 0.5 h / -25 °C

2: 130.7 mg / NaNO₂ / dimethylformamide / 18 h / 20 °C

3: 90 percent / pyridine / 6 h / 20 °C

With pyridine; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.05.085