2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

Base Information

Chemical Name:2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride
CAS No.:83436-82-2
Molecular Formula:C₁₉H₂₃NO₄*ClH
Molecular Weight:365.857
Hs Code.:

2-(2,5-dimethoxyphenyl)-ω-<N-benzyl-N-(2-hydroxyethyl)amino>acetophenone hydrochloride

Synonyms:2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

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Technology Process of 2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

There total 1 articles about 2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1204-21-3
2-bromo-2',5'-dimethoxyacetophenone

: 104-63-2
N-Benzylethanolamine

: 83436-82-2
2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

Guidance literature:: In benzene; 1.) 50 deg C, 3 h, 2.) RT, overnight;
DOI:10.1021/jm00356a026

Reference yield: 64.0%

: 83436-82-2
2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

: 83436-83-3
1-(2,5-dimethoxyphenyl)-2-ethanol hydrochloride

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In methanol; for 1h; Ambient temperature;
DOI:10.1021/jm00356a026

Reference yield:

: 83436-82-2
2-(2,5-dimethoxyphenyl)-ω-acetophenone hydrochloride

: 83436-71-9
2-(2,5-dimethoxyphenyl)morpholine

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / NaBH₄, 2 N aq. NaOH / methanol / 1 h / Ambient temperature

2: 80 percent / 6percent HCl / 2 h / Heating

3: 60 percent / H₂ / 10percent Pd/C / ethanol / 50 °C / 760 Torr

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00356a026