C₃₂H₄₃NO₄Si

Base Information

Chemical Name:C₃₂H₄₃NO₄Si
CAS No.:498542-72-6
Molecular Formula:C₃₂H₄₃NO₄Si
Molecular Weight:533.783
Hs Code.:

C<sub>32</sub>H<sub>43</sub>NO<sub>4</sub>Si

Synonyms:C₃₂H₄₃NO₄Si

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Chemical Property of C₃₂H₄₃NO₄Si

Chemical Property:

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Technology Process of C₃₂H₄₃NO₄Si

There total 9 articles about C₃₂H₄₃NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 79-22-1
methyl chloroformate

: 498542-70-4
C₃₀H₄₁NO₂Si

: 498542-72-6
C₃₂H₄₃NO₄Si

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0960-894X(02)00373-6

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 498542-72-6
C₃₂H₄₃NO₄Si

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / imidazole; 4-DMAP / CH₂Cl₂ / 20 °C

2: 100 percent / H₂ / PtO₂ / ethanol / 20 °C

3: 100 percent / LiAlH₄ / tetrahydrofuran / 20 °C

4: 100 percent / Et₃N / CH₂Cl₂ / 20 °C

5: 100 percent / BF₃*OEt₂ / diethyl ether / -78 °C

6: 95 percent / I₂; Ph₃P; imidazole / benzene / 20 °C

7: 95 percent / LDA / tetrahydrofuran / -78 °C

8: 100 percent / LDA / tetrahydrofuran / -78 °C

With 1H-imidazole; dmap; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; hydrogen; iodine; triethylamine; triphenylphosphine; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1016/S0960-894X(02)00373-6

Reference yield:

: [(1S,5S)-1-Hydroxymethyl-6-aza-spiro[4.5]dec-(7Z)-ylidene]-acetic acid ethyl ester

: 498542-72-6
C₃₂H₄₃NO₄Si

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / imidazole; 4-DMAP / CH₂Cl₂ / 20 °C

2: 100 percent / H₂ / PtO₂ / ethanol / 20 °C

3: 100 percent / LiAlH₄ / tetrahydrofuran / 20 °C

4: 100 percent / Et₃N / CH₂Cl₂ / 20 °C

5: 100 percent / BF₃*OEt₂ / diethyl ether / -78 °C

6: 95 percent / I₂; Ph₃P; imidazole / benzene / 20 °C

7: 95 percent / LDA / tetrahydrofuran / -78 °C

8: 100 percent / LDA / tetrahydrofuran / -78 °C

With 1H-imidazole; dmap; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; hydrogen; iodine; triethylamine; triphenylphosphine; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1016/S0960-894X(02)00373-6