4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate)

Base Information

• Chemical Name: 4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate)
• CAS No.: 1217038-20-4
• Molecular Formula: C₄₇H₅₄O₉SSi
• Molecular Weight: 823.092

Synonyms:4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate)

Chemical Property of 4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate)

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Technology Process of 4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate)

There total 1 articles about 4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C47H56O9SSi (1217038-05-5) → 4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate) (1217038-20-4)

Guidance literature:

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/ejoc.200901041

Reference yield: 81.0%

4-{(1R,6S)-6-(benzyloxy)-7-[4-(benzyloxy)phenyl]-1-(tert-butyldimethylsilyloxy)-3,5-dioxoheptyl}-2-methoxyphenyl-1-(4-methylbenzenesulfonate) (1217038-20-4) → 4-((R)-6-{(S)-1-(benzyloxy)-2-[4-(benzyloxy)phenyl]ethyl}-4-oxo-3,4-dihydro-2H-pyran-2-yl)-2-methoxyphenyl-1-(4-methylbenzenesulfonate) (1217038-21-5)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/ejoc.200901041

upstream raw materials:

C₄₇H₅₆O₉SSi

Downstream raw materials:

4-((R)-6-{(S)-1-(benzyloxy)-2-[4-(benzyloxy)phenyl]ethyl}-4-oxo-3,4-dihydro-2H-pyran-2-yl)-2-methoxyphenyl-1-(4-methylbenzenesulfonate)

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