dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Base Information

Chemical Name:dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate
CAS No.:210100-23-5
Molecular Formula:C₄₁H₃₇O₁₁P
Molecular Weight:736.712
Hs Code.:

Synonyms:dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Suppliers and Price of dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

There total 6 articles about dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1623-08-1
phosphoric acid dibenzyl ester

: 210100-20-2
2,4,6-tri-O-benzoyl-3-deoxy-α-L-xylo-hexopyranosyl bromide

: 210100-23-5
dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Guidance literature:: With 3 A molecular sieve; silver carbonate; In diethyl ether; dichloromethane; acetonitrile; for 18h;
DOI:10.1016/S0008-6215(97)10094-5

Reference yield:

: 210100-08-6
O²,O³,O⁵,O⁶-tetraacetyl-L-galactonic acid-lactone

: 210100-23-5
dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / Et₃N, H₂ / 3percent Pd/C / ethyl acetate / 18 h / 2280 Torr

2: 81 percent / diisoamyl borane / CH₂Cl₂ / 18 h / 0 °C

3: 0.5 g / 0.1M NaOMe / methanol / 24 h

4: 58 percent / pyridine; CH₂Cl₂ / 5 h / -40 °C

5: 63 percent / HBr / acetic acid; acetic anhydride / 2 h

6: 90 percent / molecular sieves 3 Angstroem, Ag₂CO₃ / CH₂Cl₂; acetonitrile; diethyl ether / 18 h

With diisoamyl borane; 3 A molecular sieve; hydrogen bromide; hydrogen; sodium methylate; triethylamine; silver carbonate; palladium on activated charcoal; In pyridine; methanol; diethyl ether; dichloromethane; acetic anhydride; acetic acid; ethyl acetate; acetonitrile;
DOI:10.1016/S0008-6215(97)10094-5

Reference yield:

: 79580-62-4
tri-O-acetyl-3-deoxy-D-arabino-hexono-1,4-lactone

: 210100-23-5
dibenzyl-(2,4,6-tri-O-benzoyl-3-deoxy-β-L-xylo-hexopyranosyl)-phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / diisoamyl borane / CH₂Cl₂ / 18 h / 0 °C

2: 0.5 g / 0.1M NaOMe / methanol / 24 h

3: 58 percent / pyridine; CH₂Cl₂ / 5 h / -40 °C

4: 63 percent / HBr / acetic acid; acetic anhydride / 2 h

5: 90 percent / molecular sieves 3 Angstroem, Ag₂CO₃ / CH₂Cl₂; acetonitrile; diethyl ether / 18 h

With diisoamyl borane; 3 A molecular sieve; hydrogen bromide; sodium methylate; silver carbonate; In pyridine; methanol; diethyl ether; dichloromethane; acetic anhydride; acetic acid; acetonitrile;
DOI:10.1016/S0008-6215(97)10094-5