Technology Process of C23H34O6
There total 5 articles about C23H34O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tri-sec-butyl-borohydride;
In
tetrahydrofuran;
at -78 ℃;
for 1.08333h;
Inert atmosphere;
DOI:10.1021/jo2010389
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: cerium(III) chloride heptahydrate / methanol / 0.75 h / 20 °C / Inert atmosphere
1.2: 1.08 h / -78 °C / Inert atmosphere
1.3: 0 - 20 °C / Inert atmosphere
2.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
3.1: potassium tri-sec-butyl-borohydride / tetrahydrofuran / 1.08 h / -78 °C / Inert atmosphere
With
cerium(III) chloride heptahydrate; potassium tri-sec-butyl-borohydride;
In
tetrahydrofuran; methanol;
DOI:10.1021/jo2010389
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / acetonitrile / 0.75 h / 20 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
2.1: cerium(III) chloride heptahydrate / methanol / 0.75 h / 20 °C / Inert atmosphere
2.2: 1.08 h / -78 °C / Inert atmosphere
2.3: 0 - 20 °C / Inert atmosphere
3.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
4.1: potassium tri-sec-butyl-borohydride / tetrahydrofuran / 1.08 h / -78 °C / Inert atmosphere
With
cerium(III) chloride heptahydrate; potassium tri-sec-butyl-borohydride; caesium carbonate;
In
tetrahydrofuran; methanol; acetonitrile;
1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jo2010389
