5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

Base Information

Chemical Name:5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one
CAS No.:300809-98-7
Molecular Formula:C₁₉H₃₁NO₂Si₂
Molecular Weight:361.632
Hs Code.:

5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3<i>H</i>-furan-2-one

Synonyms:5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

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Chemical Property of 5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

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Technology Process of 5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

There total 1 articles about 5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5933-40-4
(R)-(+)-N,α-dimethylbenzylamine

: 145178-53-6
2,3-bis(trimethylsilyl)-1,3-butadiene-1,4-dione

: 300809-98-7
5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

Guidance literature:: In dichloromethane; at -78 ℃; for 1h;
DOI:10.1021/jo000508k

Reference yield:

: 300809-98-7
5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

: Methyl-((R)-1-phenyl-ethyl)-(3-trimethylsilanyl-5-trimethylsilanyloxy-furan-2-yl)-amine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 0.25h;
DOI:10.1021/jo000508k

Reference yield:

: 300809-98-7
5-[methyl-(1-phenyl-ethyl)-amino]-3,4-bis-trimethylsilanyl-3H-furan-2-one

: C₁₃H₂₁N₃O₆SiC₉H₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: TMSOTf / CH₂Cl₂ / 0.25 h

2: CH₂Cl₂

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; 1: Isomerization / 2: Addition;
DOI:10.1021/jo000508k