(3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

Base Information

Chemical Name:(3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine
CAS No.:1428558-83-1
Molecular Formula:C₄₀H₅₅N₃O₂
Molecular Weight:609.896
Hs Code.:

(3R,4R)-N<sub>3</sub>,N<sub>4</sub>-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

Synonyms:(3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

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Chemical Property of (3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

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Technology Process of (3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

There total 4 articles about (3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 880497-74-5
(3R,4R)-3,4-diamino-1-phenylpyrrolidine

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 1428558-83-1
(3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

Guidance literature:: With silica gel; In dichloromethane; for 0.5h; Sonication;
DOI:10.1016/j.tetasy.2013.01.015

Reference yield:

: 62-53-3
aniline

: 1428558-83-1
(3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 5,5-dimethyl-1,3-cyclohexadiene / Reflux

2.1: Reflux

3.1: lithium aluminium tetrahydride / diethyl ether / Reflux

3.2: 20 °C

4.1: silica gel / dichloromethane / 0.5 h / Sonication

With lithium aluminium tetrahydride; silica gel; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; dichloromethane;
DOI:10.1016/j.tetasy.2013.01.015

Reference yield:

: 69669-21-2
(3R,4R)-1-phenyl-3,4-dihydroxy-2,5-dioxopyrrolidine

: 1428558-83-1
(3R,4R)-N₃,N₄-bis[3,5-di-t-butylsalicylidene]-1-phenyl-3,4-diaminopyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: Reflux

2.1: lithium aluminium tetrahydride / diethyl ether / Reflux

2.2: 20 °C

3.1: silica gel / dichloromethane / 0.5 h / Sonication

With lithium aluminium tetrahydride; silica gel; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetasy.2013.01.015