Tungsten, (h6-benzene)tricarbonyl-

Base Information

Chemical Name:Tungsten, (h6-benzene)tricarbonyl-
CAS No.:12128-53-9
Molecular Formula:C9H6 O3 W
Molecular Weight:345.995
Hs Code.:

Synonyms:Benzenetungstentricarbonyl (6CI); Tungsten, (benzene)tricarbonyl- (7CI,8CI); Benzene, tungstencomplex; (Benzene)tricarbonyltungsten; (h6-Benzene)tricarbonyltungsten; (h6-Benzene)tungsten tricarbonyl

Suppliers and Price of Tungsten, (h6-benzene)tricarbonyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Tungsten, (h6-benzene)tricarbonyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Tungsten, (h6-benzene)tricarbonyl-

There total 2 articles about Tungsten, (h6-benzene)tricarbonyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 115677-62-8
(tungstenpentacarbonyl)2(μ-CH3OCCH(C3H7)CH2C(CH3)(CH2CHCH2)COCH3)

: 14040-11-0
tungsten hexacarbonyl

: 12128-53-9
(η(6)-benzene)tungsten(0) tricarbonyl

: C(CH₃)(CH₂CHCH₂)C(OCH₃)C(OCH₃)CH(C₂H₄CH₃)CH₂

Guidance literature:: In benzene-d6; heating 3 h in benzene at 75°C; identification of organometallic products by (13)C NMR;

Reference yield: 27.0%

: 81097-61-2
fac-W(CO)3(PMTA)

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 12128-53-9
(η(6)-benzene)tungsten(0) tricarbonyl

: W(CO)4(PMTA)

: 3030-47-5
N,N,N',N'',N'''-pentamethyldiethylenetriamine

Guidance literature:: In benzene; Schlenk techniques used; protective gas: N2; detailed description given; to stirred soln. of W(CO)3PMTA in benzene, BF3*OEt2 was added; reflux (2 h); cooling to room temp.;; filtration; evapn. to dryness; filtration of residue (through alumina/CH2Cl2 - hexane 1:4); 1. fraction (W(CO)6C6H6: evapn.; recrystn. (CH2Cl2/pentane/-20°C); 2. fraction (W(CO)4PMTA): evapn.; recrystn. (CH2Cl2/hexane/-20°C); elem. anal.;;
DOI:10.1016/0022-328X(91)86100-5