isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside
CAS No.:401592-98-1
Molecular Formula:C₄₈H₅₄O₇SSi
Molecular Weight:803.104
Hs Code.:

Synonyms:isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

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Chemical Property of isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

Chemical Property:

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Technology Process of isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

There total 4 articles about isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-83-5
trityl chloride

: 401592-98-1
isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; DMAP / 16 h / 80 °C

2: imidazole / dimethylformamide / 4 h / 20 °C

3: 1.65 g / pyridine / 24 h / 50 °C

With pyridine; 1H-imidazole; dmap; In N,N-dimethyl-formamide;
DOI:10.1039/b108399f

Reference yield:

: 367-93-1
isopropyl β-D-thiogalactopyranoside

: 401592-98-1
isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; DMAP / 16 h / 80 °C

2: imidazole / dimethylformamide / 4 h / 20 °C

3: 1.65 g / pyridine / 24 h / 50 °C

With pyridine; 1H-imidazole; dmap; In N,N-dimethyl-formamide;
DOI:10.1039/b108399f

Reference yield:

: 669695-14-1
(2S,3R,4S,5R,6R)-2-Isopropylsulfanyl-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

: 401592-98-1
isopropyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 4 h / 20 °C

2: 1.65 g / pyridine / 24 h / 50 °C

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1039/b108399f