bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

Base Information

Chemical Name:bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane
CAS No.:635724-04-8
Molecular Formula:C₃₇H₂₆N₂O₃
Molecular Weight:546.625
Hs Code.:

Synonyms:bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

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Chemical Property of bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

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Technology Process of bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

There total 3 articles about bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 635723-98-7
α,α-bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)-1,4-benzoquinonemethide

: 635724-04-8
bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

Guidance literature:: With hydrogenchloride; acetic acid; zinc; at 80 ℃; for 8h;
DOI:10.1246/bcsj.76.2035

Reference yield: 92.0%

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 303730-52-1
1,2-Dihydro-N-phenylcyclohepta[b]pyrrol-2-one

: 635724-04-8
bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

Guidance literature:: With trifluoroacetic acid; In chloroform; at 80 ℃; for 6h;
DOI:10.1246/bcsj.76.2035

Reference yield:

: 4-acetoxyphenyl-bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl tetrafluoroborate

: 635724-04-8
bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)(4-hydroxyphenyl)methane

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / K₂CO₃ / CH₂Cl₂ / 48 h / 20 °C

2: 100 percent / Zn; AcOH; aq. HCl / 8 h / 80 °C

With hydrogenchloride; potassium carbonate; acetic acid; zinc; In dichloromethane;
DOI:10.1246/bcsj.76.2035