Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline

Base Information

• Chemical Name: Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline
• CAS No.: 82500-97-8
• Molecular Formula: C₁₆H₁₆N₄O
• Molecular Weight: 280.329
• Mol file: 82500-97-8.mol

Synonyms:Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline

Chemical Property of Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline

There total 4 articles about Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Chloro-2 (o-methoxybenzyl)-3 quinoxaline (82500-95-6) → Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline (82500-97-8)

Guidance literature:

With hydrazine hydrate; In methanol; for 1h; Heating;

Reference yield:

Acide o-methoxyphenylpyruvique (82204-44-2) → Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline (82500-97-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 87 percent / Acide acetique / ethanol / 0.5 h / Heating

2: 88 percent / POCl₃, pyridine / 1 h / Heating

3: 80 percent / Nh₂NH₂*H₂O / methanol / 1 h / Heating

With pyridine; hydrazine hydrate; acetic acid; trichlorophosphate; In methanol; ethanol;

Reference yield:

(o-methoxybenzyl)-3 1H-quinoxalinone-2 (82500-92-3) → Hydrazino-2 (o-methoxybenzyl)-3 quinoxaline (82500-97-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / POCl₃, pyridine / 1 h / Heating

2: 80 percent / Nh₂NH₂*H₂O / methanol / 1 h / Heating

With pyridine; hydrazine hydrate; trichlorophosphate; In methanol;

upstream raw materials:

Chloro-2 (o-methoxybenzyl)-3 quinoxaline

Acide o-methoxyphenylpyruvique

(o-methoxybenzyl)-3 1H-quinoxalinone-2

1,2-diamino-benzene

Downstream raw materials:

(o-methoxybenzyl)-3 quinoxaline