diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

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Chemical Name:diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate
CAS No.:376395-35-6
Molecular Formula:C₂₈H₃₉NO₆
Molecular Weight:485.621
Hs Code.:

Synonyms:diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

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Technology Process of diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

There total 4 articles about diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1026558-61-1
methanesulfonic acid 4-ethyl-2-methanesulfonyloxymethyl-octyl ester

: 376395-32-3
diethyl 1-benzyl-3,4-dihydroxy-1H-pyrrole-2,5-dicarboxylate

: 376395-35-6
diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 12h;
DOI:10.1021/jo001620l

Reference yield:

: 18908-66-2
3-bromomethylheptane

: 376395-35-6
diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / NaOEt / ethanol / 6 h / 20 °C

2: 70 percent / LiAlH₄ / diethyl ether / 6 h / 20 °C

3: triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / 20 °C

4: 71 percent / K₂CO₃ / dimethylformamide / 12 h / 110 °C

With dmap; lithium aluminium tetrahydride; sodium ethanolate; potassium carbonate; triethylamine; In diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo001620l

Reference yield:

: 24306-19-2
diethyl 2-(2-ethylhexyl)malonate

: 376395-35-6
diethyl N-benzyl-3,4-[2-(2-ethylhexyl)-1,3-propylenedioxy]pyrrole-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / LiAlH₄ / diethyl ether / 6 h / 20 °C

2: triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / 20 °C

3: 71 percent / K₂CO₃ / dimethylformamide / 12 h / 110 °C

With dmap; lithium aluminium tetrahydride; potassium carbonate; triethylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo001620l