Technology Process of C26H32O2
There total 6 articles about C26H32O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
for 2h;
DOI:10.1021/ja063384n
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: DIBAL-H / diethyl ether; petroleum ether / -78 - 0 °C
2.1: Et3N / CH2Cl2 / 1 h / 0 °C
3.1: LDA / tetrahydrofuran; petroleum ether / 1 h / -78 °C
3.2: 75 percent / tetrahydrofuran; petroleum ether / 2.5 h / 0 - 20 °C
4.1: DIBAL-H / diethyl ether; petroleum ether / -78 - 0 °C
5.1: oxalyl chloride; methyl sulfoxide; Et3N / CH2Cl2 / -78 - 20 °C
6.1: 85 percent / K2CO3 / methanol / 0 - 20 °C
7.1: 72 percent / Et3N / PdCl2(PPh3)2; CuI / 2 h
With
oxalyl dichloride; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; Petroleum ether;
5.1: Swern oxidation / 7.1: Sonogashira cross-coupling;
DOI:10.1021/ja063384n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / K2CO3 / methanol / 0 - 20 °C
2: 72 percent / Et3N / PdCl2(PPh3)2; CuI / 2 h
With
potassium carbonate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
methanol;
2: Sonogashira cross-coupling;
DOI:10.1021/ja063384n
