Technology Process of 1-cyclopentyl-2-isothiocyanatobenzene
There total 4 articles about 1-cyclopentyl-2-isothiocyanatobenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
dichloromethane; water;
at 20 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / water; 1,4-dioxane / 80 °C / Inert atmosphere
2: hydrogen; 5%-palladium/activated carbon / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere
3: sodium hydrogencarbonate / water; dichloromethane / 1 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; 5%-palladium/activated carbon; hydrogen; sodium hydrogencarbonate; sodium carbonate;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / water; 1,4-dioxane / 80 °C / Inert atmosphere
2: hydrogen; 5%-palladium/activated carbon / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere
3: sodium hydrogencarbonate / water; dichloromethane / 1 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; 5%-palladium/activated carbon; hydrogen; sodium hydrogencarbonate; sodium carbonate;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;
