C₁₃H₁₈O₃

Base Information

Chemical Name:C₁₃H₁₈O₃
CAS No.:949932-83-6
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:

C<sub>13</sub>H<sub>18</sub>O<sub>3</sub>

Synonyms:C₁₃H₁₈O₃

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Chemical Property of C₁₃H₁₈O₃

Chemical Property:

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Technology Process of C₁₃H₁₈O₃

There total 11 articles about C₁₃H₁₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 949932-60-9
C₂₀H₂₄O₅S

: 949932-83-6
C₁₃H₁₈O₃

Guidance literature:: With sodium amalgam; In tetrahydrofuran; methanol; at 20 ℃; for 2h;
DOI:10.1021/ol071176+

Reference yield:

: 949932-74-5
C₂₂H₂₆SO₅

: 949932-83-6
C₁₃H₁₈O₃

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / K₂CO₃ / methanol / 1 h / 20 °C

2: Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

3: 96 mg / SmI₂ / tetrahydrofuran; methanol / 0.17 h / 0 °C

4: 100 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

5: 69 percent / sodium amalgam / methanol; tetrahydrofuran / 2 h / 20 °C

With sodium amalgam; samarium diiodide; potassium carbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1021/ol071176+

Reference yield:

: 949932-78-9
C₂₀H₂₄O₄S

: 949932-83-6
C₁₃H₁₈O₃

Guidance literature:: Multi-step reaction with 4 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

2: 116 mg / SmI₂ / tetrahydrofuran; methanol / 0.17 h / 0 °C

3: 90 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

4: 69 percent / sodium amalgam / methanol; tetrahydrofuran / 2 h / 20 °C

With sodium amalgam; samarium diiodide; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; 1: Dess-Martin oxidation;
DOI:10.1021/ol071176+