3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

Base Information

Chemical Name:3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine
CAS No.:1395729-02-8
Molecular Formula:C₃₁H₂₉FIN
Molecular Weight:561.481
Hs Code.:

Synonyms:3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

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Technology Process of 3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

There total 2 articles about 3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1395727-01-1
7-fluoro-4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinoline

: 1395729-02-8
3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

Guidance literature:: With Iodine monochloride; In dichloromethane; acetonitrile; at 0 ℃; for 0.416667h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.07.067

Reference yield:

: 183210-84-6
1,4-bis(4-tert-butylphenyl)buta-1,3-diyne

: 1395729-02-8
3-fluoro-7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-butylamine / N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere

1.2: 28 h / 120 °C / Inert atmosphere

2.1: Iodine monochloride / dichloromethane; acetonitrile / 0.42 h / 0 °C / Inert atmosphere

With Iodine monochloride; tert-butylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.07.067