C₂₉H₄₅O₉PSi

Base Information

Chemical Name:C₂₉H₄₅O₉PSi
CAS No.:1338989-64-2
Molecular Formula:C₂₉H₄₅O₉PSi
Molecular Weight:596.73
Hs Code.:

C<sub>29</sub>H<sub>45</sub>O<sub>9</sub>PSi

Synonyms:C₂₉H₄₅O₉PSi

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Chemical Property of C₂₉H₄₅O₉PSi

Chemical Property:

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Technology Process of C₂₉H₄₅O₉PSi

There total 14 articles about C₂₉H₄₅O₉PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₆O₆Si

: 756-79-6
dimethyl methane phosphonate

: 1338989-64-2
C₂₉H₄₅O₉PSi

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; at -78 ℃;

C₂₆H₃₆O₆Si; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: 1338989-47-1
C₁₃H₁₇NO₄

: 1338989-64-2
C₂₉H₄₅O₉PSi

Guidance literature:: Multi-step reaction with 10 steps

1: tert.-butyl lithium / tetrahydrofuran / -78 °C

2: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C

3: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C

4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C

6: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C

7: 2,6-dimethylpyridine / dichloromethane / -40 °C

8: methanol; potassium carbonate / -15 °C

9: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 24 °C

10: n-butyllithium / tetrahydrofuran / -78 °C

With 2,6-dimethylpyridine; methanol; tert.-butylhydroperoxide; lithium aluminium tetrahydride; n-butyllithium; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane; 9: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: C₂₁H₃₂O₄Si

: 1338989-64-2
C₂₉H₄₅O₉PSi

Guidance literature:: Multi-step reaction with 9 steps

1: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C

2: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C

3: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C

6: 2,6-dimethylpyridine / dichloromethane / -40 °C

7: methanol; potassium carbonate / -15 °C

8: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 24 °C

9: n-butyllithium / tetrahydrofuran / -78 °C

With 2,6-dimethylpyridine; methanol; tert.-butylhydroperoxide; lithium aluminium tetrahydride; n-butyllithium; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane; 8: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.08.051