methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

Base Information

Chemical Name:methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate
CAS No.:1027223-95-5
Molecular Formula:C₁₄H₁₂INO
Molecular Weight:337.16
Hs Code.:

Synonyms:methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

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Technology Process of methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

There total 1 articles about methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 615-43-0
2-iodophenylamine

: 707-07-3
orthobenzoic acid trimethyl ester

: 1027223-95-5
methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/adsc.201400072

Reference yield: 99.0%

: 1027223-95-5
methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

: 1066-54-2
trimethylsilylacetylene

: methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201400072

Reference yield:

: 1027223-95-5
methyl (Z)-N-{2-[(trimethylsilyl)ethynyl]phenyl}benzimidate

: 536-74-3
phenylacetylene

: C₂₂H₁₇NO

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; Inert atmosphere;
DOI:10.1021/ol800202u