Technology Process of C49H79NO14S
There total 8 articles about C49H79NO14S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol;
at 70 ℃;
for 8h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol / 30 h / 40 °C
2.1: dichloromethane / 5 h / 25 °C
3.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
3.2: 2 h / 0 - 10 °C
4.1: silver(I) chloride / methanol / 4 h / 20 °C
4.2: 19 h / 20 - 90 °C / Inert atmosphere
5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol / 8 h / 70 °C
With
methanol; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; silver(I) chloride;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide / acetone / 2.5 h / 20 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 5 °C / Inert atmosphere; Ice cooling
3.1: methanol / 30 h / 40 °C
4.1: dichloromethane / 5 h / 25 °C
5.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
5.2: 2 h / 0 - 10 °C
6.1: silver(I) chloride / methanol / 4 h / 20 °C
6.2: 19 h / 20 - 90 °C / Inert atmosphere
7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol / 8 h / 70 °C
With
methanol; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; silver(I) chloride;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; mineral oil;