Technology Process of C32H21N3O2
There total 7 articles about C32H21N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium phosphate; copper(l) iodide; trans cyclohexane-1,2-diamine;
In
1,4-dioxane;
at 120 ℃;
for 10h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
1.2: 1.5 h / 20 °C / Inert atmosphere
2.1: N-Bromosuccinimide / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 °C / Inert atmosphere
3.2: 1 h
4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene; ethanol / 90 °C
5.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 1 h / 20 °C
6.1: copper(l) iodide; potassium phosphate; trans cyclohexane-1,2-diamine / 1,4-dioxane / 10 h / 120 °C
With
potassium phosphate; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; trans cyclohexane-1,2-diamine; sodium hydride; sodium carbonate; tetra-n-butylammoniumfluoride trihydrate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; hexane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 °C / Inert atmosphere
1.2: 1 h
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene; ethanol / 90 °C
3.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 1 h / 20 °C
4.1: copper(l) iodide; potassium phosphate; trans cyclohexane-1,2-diamine / 1,4-dioxane / 10 h / 120 °C
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; trans cyclohexane-1,2-diamine; sodium carbonate; tetra-n-butylammoniumfluoride trihydrate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; hexane; water; toluene;