2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1594137-50-4
• Molecular Formula: C₂₂H₂₄BF₂IN₂
• Molecular Weight: 492.158

Synonyms:2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 1 articles about 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5,5-difluoro-10-mesityl-1,3,7,9-tetramethyl-5H-4λ4,5λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine (1308671-66-0) → 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1594137-50-4)

Guidance literature:

With iodine; iodic acid; In ethanol; dichloromethane; water; at 65 ℃; for 1h;

DOI:10.1002/chem.201303468

Reference yield: 94.0%

2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1594137-50-4) + 1-propynyltributylstannane (64099-82-7) → 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1594137-51-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 95 ℃; for 4h;

DOI:10.1002/chem.201303468

Reference yield: 93.0%

2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1594137-50-4) + 4-Tributylstannanyl-benzoic acid benzyl ester (134078-93-6) → C36H35BF2N2O2

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; for 24h;

DOI:10.1002/zaac.201500695

upstream raw materials:

5,5-difluoro-10-mesityl-1,3,7,9-tetramethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

Downstream raw materials:

C₃₀H₃₁BF₂N₂

C₄₆H₄₈B₂F₄N₄

2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

8-mesityl-1,3,5,7-tetramethyl-2-vinyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1594137-50-4 2-iodo-8-mesityl-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Send

Send

Metric Ton KG G Pound L ML

Send

Send