C₂₇H₃₇NO₅

Base Information Edit

Chemical Name:C₂₇H₃₇NO₅
CAS No.:943542-45-8
Molecular Formula:C₂₇H₃₇NO₅
Molecular Weight:455.594
Hs Code.:
Mol file:943542-45-8.mol

C<sub>27</sub>H<sub>37</sub>NO<sub>5</sub>

Synonyms:C₂₇H₃₇NO₅

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Chemical Property of C₂₇H₃₇NO₅ Edit

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Technology Process of C₂₇H₃₇NO₅

There total 8 articles about C₂₇H₃₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.4%

: 943542-46-9
C₂₁H₂₇NO₅

: 61967-15-5
9-cyclohex-2-enyl-9-borabicyclo[3.3.1]nonane

: 943542-45-8
C₂₇H₃₇NO₅

Guidance literature:: C₂₁H₂₇NO₅; 9-cyclohex-2-enyl-9-borabicyclo[3.3.1]nonane; In tetrahydrofuran; at -78 - 20 ℃; for 11.5h;

With ethanolamine; In tetrahydrofuran; at 20 ℃; for 8h; Further stages.;
DOI:10.1021/ol0706051

Reference yield:

: 943542-62-9
C₂₁H₂₉NO₅

: 943542-45-8
C₂₇H₃₇NO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3.9 g / NMO; TPAP / CH₂Cl₂ / 18 h / 20 °C

2.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

2.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0706051

Reference yield:

: 943542-50-5
C₁₅H₂₃NO₆

: 943542-45-8
C₂₇H₃₇NO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: 8.8 g / t-BuOK / tetrahydrofuran / 6 h / 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: tetrahydrofuran; methanol / 24 h / 20 °C

3.1: 3.9 g / NMO; TPAP / CH₂Cl₂ / 18 h / 20 °C

4.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

4.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

With lithium borohydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; potassium tert-butylate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0706051