2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester

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Chemical Name:2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester
CAS No.:186038-44-8
Molecular Formula:C₂₈H₃₉BrO₆
Molecular Weight:551.518
Hs Code.:

Synonyms:2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester

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Chemical Property of 2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester

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Technology Process of 2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester

There total 1 articles about 2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 91739-72-9
Trans-p-Menthane-3,8-diol

: 2-bromo-4,4-bis(ethoxycarbonyl)-6,6-diethoxy-1-phenyl-1-hexene

: 186038-44-8
2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester

Guidance literature:: With camphor-10-sulfonic acid; In toluene; for 2h; Heating;
DOI:10.1021/jo961750n

Reference yield: 65.0%

: 186038-44-8
2-((E)-2-Bromo-3-phenyl-allyl)-2-((2R,4aR,7R,8aR)-4,4,7-trimethyl-hexahydro-benzo[1,3]dioxin-2-ylmethyl)-malonic acid diethyl ester

: C₂₈H₄₀O₆

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tributyltin chloride; sodium cyanoborohydride; In tert-butyl alcohol; at 80 ℃; for 5h;
DOI:10.1021/jo961750n