bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester

Base Information

• Chemical Name: bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester
• CAS No.: 724785-15-3
• Molecular Formula: C₁₃H₂₀O₄
• Molecular Weight: 240.299

Synonyms:bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester

Chemical Property of bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester

Chemical Property:

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Technology Process of bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester

There total 4 articles about bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5-norbornene-endo-2-carboxylic acid (934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1) + (Z)-hex-3-en-3-yl bicyclo[2.2.1]hept-5-ene-2-carboxylate + bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester (724785-15-3)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 25 ℃; for 5h;

DOI:10.1039/c5ra04860e

Reference yield: 85.0%

5-norbornene-endo-2-carboxylic acid (934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1) + 6-(3,3-dimethylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-1-yl)hexan-1-ol + 5-norbornene-endo-2-carboxylic acid (934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1) + (Z)-hex-3-en-3-yl bicyclo[2.2.1]hept-5-ene-2-carboxylate + bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester (724785-15-3) + bicyclo[2.2.1]hept-5-en-2-yl isocyanate + 6-(3,3-dimethylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-1-yl)hexyl bicyclo[2.2.1]hept-5-ene-2-carboxylate

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 25 ℃; for 5h;

DOI:10.1039/c5ra04860e

Reference yield: 85.0%

5-norbornene-endo-2-carboxylic acid (934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1) + 6-(3,3-dimethylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-1-yl)hexan-1-ol + 5-norbornene-endo-2-carboxylic acid (934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1) + 1'-[6-hydroxyhexyl]-3',3',-dimethyl-6-nitrospiro[2H-1-benzopyran-2,2'-indoline] (129334-17-4) + 5-norbornene-endo-2-carboxylic acid (934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1) + (Z)-hex-3-en-3-yl bicyclo[2.2.1]hept-5-ene-2-carboxylate + bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 3-hydroxy-2-hydroxymethyl-2-methyl-propyl ester (724785-15-3) + bicyclo[2.2.1]hept-5-en-2-yl isocyanate + 6-(3,3-dimethylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-1-yl)hexyl bicyclo[2.2.1]hept-5-ene-2-carboxylate + bicyclo[2.2.1]hept-5-en-2-yl isocyanate

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 25 ℃; for 5h;

DOI:10.1039/c5ra04860e

upstream raw materials:

5-norbornene-endo-2-carboxylic acid

1'-[6-hydroxyhexyl]-3',3',-dimethyl-6-nitrospiro[2H-1-benzopyran-2,2'-indoline]

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