methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate

Base Information

• Chemical Name: methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate
• CAS No.: 1045792-85-5
• Molecular Formula: C₂₁H₂₇N₃O₆
• Molecular Weight: 417.462

Synonyms:methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate

Chemical Property of methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate

Chemical Property:

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Technology Process of methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate

There total 1 articles about methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(3-tert-butoxycarbonylaminophenyl)isoxazole-3-carboxylic acid + 5-aminopentanoic acid methyl ester hydrochloride (29840-56-0) → methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate (1045792-85-5)

Guidance literature:

5-(3-tert-butoxycarbonylaminophenyl)isoxazole-3-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

5-aminopentanoic acid methyl ester hydrochloride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1021/jm8002894

Reference yield: 15.0%

methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate (1045792-85-5) → C20H26N4O6 (1045792-60-6)

Guidance literature:

With potassium hydroxide; hydroxylamine hydrochloride; In methanol; at 20 ℃; for 0.5h;

DOI:10.1021/jm8002894

Reference yield:

methyl 5-[5-(3-tert-butoxycarbonylaminophenyl)-3-isoxazolecarboxamido]pentanoate (1045792-85-5) → C16H19N3O4

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm8002894

upstream raw materials:

5-aminopentanoic acid methyl ester hydrochloride

Downstream raw materials:

C₂₀H₂₆N₄O₆

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