C₅₂H₉₄O₁₀Si₂NI

Base Information

Chemical Name:C₅₂H₉₄O₁₀Si₂NI
CAS No.:930803-68-2
Molecular Formula:C₅₂H₉₄INO₁₀Si₂
Molecular Weight:1076.39
Hs Code.:

C<sub>52</sub>H<sub>94</sub>O<sub>10</sub>Si<sub>2</sub>NI

Synonyms:C₅₂H₉₄O₁₀Si₂NI

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₉₄O₁₀Si₂NI

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Technology Process of C₅₂H₉₄O₁₀Si₂NI

There total 36 articles about C₅₂H₉₄O₁₀Si₂NI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 930803-39-7
C₅₁H₉₃O₁₁Si₂N

: 75-47-8
iodoform

: 930803-68-2
C₅₂H₉₄O₁₀Si₂NI

Guidance literature:: With chromium dichloride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-25-1
C₁₀H₁₅S₂O₂Br

: 930803-68-2
C₅₂H₉₄O₁₀Si₂NI

Guidance literature:: Multi-step reaction with 11 steps

1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

2: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

3: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

4: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

5: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

6: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

7: 84 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

8: 84 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / -5 °C

9: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 20 °C / pH 7

10: 99 percent / (COCl)2; dimethyl sulfoxide; triethylamine / CH₂Cl₂

11: 82 percent / CrCl₂ / tetrahydrofuran / 0 - 20 °C

With 2,6-dimethylpyridine; chromium dichloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; oxalyl dichloride; tert.-butyl lithium; diisobutylaluminium hydride; lithium triethylborohydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 10: Swern oxidation;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-26-2
C₉H₁₅S₂OBr

: 930803-68-2
C₅₂H₉₄O₁₀Si₂NI

Guidance literature:: Multi-step reaction with 10 steps

1: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

2: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

3: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

4: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

5: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

6: 84 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

7: 84 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / -5 °C

8: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 20 °C / pH 7

9: 99 percent / (COCl)2; dimethyl sulfoxide; triethylamine / CH₂Cl₂

10: 82 percent / CrCl₂ / tetrahydrofuran / 0 - 20 °C

With 2,6-dimethylpyridine; chromium dichloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; oxalyl dichloride; tert.-butyl lithium; lithium triethylborohydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 9: Swern oxidation;
DOI:10.1002/anie.200604053