N(CH₂CH₂NC₆F₅)3Mo(Cl)

Base Information

Chemical Name:N(CH₂CH₂NC₆F₅)3Mo(Cl)
CAS No.:155019-63-9
Molecular Formula:C₂₄H₁₂ClF₁₅MoN₄
Molecular Weight:772.755
Hs Code.:

N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)3Mo(Cl)

Synonyms:N(CH₂CH₂NC₆F₅)3Mo(Cl)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N(CH₂CH₂NC₆F₅)3Mo(Cl)

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Technology Process of N(CH₂CH₂NC₆F₅)3Mo(Cl)

There total 2 articles about N(CH₂CH₂NC₆F₅)3Mo(Cl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 16998-75-7
tetrachlorobis(tetrahydrofurano)molybdenum(IV)

: 155019-77-5
2,2',2''-tris<(pentafluorophenyl)amino>triethylamine

: 155019-63-9
Mo(N(CH₂CH₂NC₆F₅)3)Cl

Guidance literature:: With N(C₂H₅)3; In tetrahydrofuran; under exclusion of air; a soln. of the amine and Et3N in THF was added to a suspn. of the Mo compd., stirred at room temp. for 3 h; filtered, extd. with THF, solvent was removed in vac., taken up in 1,2-dimethoxyethane, filtered, solvent was removed in vac., washed with pentane, recrystd. from THF-ether; elem. anal.;
DOI:10.1021/ja00089a028

Reference yield: 33.0%

: 155019-61-7
Mo(N(CH₂CH₂NC₆F₅)3)(N(CH₃)2)

: 155019-63-9
Mo(N(CH₂CH₂NC₆F₅)3)Cl

Guidance literature:: With HCl; In diethyl ether; byproducts: NH2(CH3)2Cl; under exclusion of air; a soln. of HCl in ether was added to a precooled soln. of the Mo compd., stirred at room temp. overnight; filtered, washed with CH2Cl2, ether, pentane, dried under vac.;
DOI:10.1021/ja00089a028

Reference yield: 81.0%

: 155019-63-9
Mo(N(CH₂CH₂NC₆F₅)3)Cl

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 155019-65-1
((C₆F₅NCH₂CH₂)3N)MoOTf

Guidance literature:: In dichloromethane; under exclusion of air; the triflate was added to a soln. of complex in CH2Cl2, stirred at room temp. for 2 d; filtered, washed with CH2Cl2 and pentane, dried under vac.; elem. anal.;
DOI:10.1021/ja00089a028