N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

Base Information

Chemical Name:N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester
CAS No.:107033-41-0
Molecular Formula:C₃₂H₄₀N₄O₉S
Molecular Weight:656.757
Hs Code.:

Synonyms:N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

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Chemical Property of N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

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Technology Process of N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

There total 8 articles about N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106947-94-8
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

: 63092-05-7
L-Alanyl-D-isoglutamin-γ-benzylester-hydrochlorid

: 107033-41-0
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 106947-89-1
Methyl-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-β-D-glucofuranosid

: 107033-41-0
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

Guidance literature:: Multi-step reaction with 7 steps

1: 58 percent / DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

2: 58 percent / pyridine / 16 h / -10 °C

3: 54 percent / pyridine / 16 h / Ambient temperature

4: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

5: 45 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 5 h

6: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 40 °C

7: 62 percent / Et₃N / dimethylformamide / 1 h / Ambient temperature

With pyridine; dmap; sodium methylate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 3804-93-1
(R)-2-[(3aR,5S,6R,6aR)-5-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazol-6-yloxy]-propionic acid

: 107033-41-0
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

Guidance literature:: Multi-step reaction with 9 steps

1: 87 percent / 168 h / Ambient temperature

2: 86 percent / 60percent aq. CH₃COOH / 23 h / Ambient temperature

3: 58 percent / DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

4: 58 percent / pyridine / 16 h / -10 °C

5: 54 percent / pyridine / 16 h / Ambient temperature

6: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

7: 45 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 5 h

8: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 40 °C

9: 62 percent / Et₃N / dimethylformamide / 1 h / Ambient temperature

With pyridine; dmap; sodium methylate; acetic acid; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide;